Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester → N-(3-Amino[1,1'-biphenyl]-4-yl)-carbamic Acid tert-Butyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester | HCID 57745588 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | N-(3-Amino[1,1'-biphenyl]-4-yl)-carbamic Acid tert-Butyl Ester | HCID 57717454 | 93.4% |
반응 단계
Prepared from (3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example B5) (100 mg, 0.32 mmol) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a white solid (85 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06509328B1 |
| 출처 데이터셋 | uspto-grants-2003_01 |
| ORD ID | ord-7da7550c2dc742c3a7a5df193010206e |
| 출처 메모 | uspto-grants-2003_01 |