2-(9H-carbazol-2-yloxy)ethylamine → HCID 18615263, 화합물

HRID 1636949노트

반응식

HRID 1636949 반응식
Br[CH2:2][C:3]([C:5]1[CH:10]=[C:9]([NH:11][S:12]([CH3:15])(=[O:14])=[O:13])[CH:8]=[C:7]([O:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:6]=1)=[O:4].[CH:24]1[C:36]2[NH:35][C:34]3[C:29](=[CH:30][CH:31]=[CH:32][CH:33]=3)[C:28]=2[CH:27]=[CH:26][C:25]=1[O:37][CH2:38][CH2:39][NH2:40]>CO.C(Cl)(Cl)Cl>[CH:24]1[C:36]2[NH:35][C:34]3[C:29](=[CH:30][CH:31]=[CH:32][CH:33]=3)[C:28]=2[CH:27]=[CH:26][C:25]=1[O:37][CH2:38][CH2:39][NH:40][CH2:2][CH:3]([C:5]1[CH:6]=[C:7]([O:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:8]=[C:9]([NH:11][S:12]([CH3:15])(=[O:14])=[O:13])[CH:10]=1)[OH:4]

참가 물질

4

반응물 2

HCID 110854932-(9H-carbazol-2-yloxy)ethylamineHCID 18615151HCID 18615151, 화합물

생성물 1

HCID 18615263HCID 18615263, 화합물

시약·촉매·용매 1

HCID 21584188Chloroform methanol용매

실험 절차

170 mg of Intermediate 62 and 95 mg of Intermediate 2. Rf=0.28 (methanol/chloroform of 1/9).

출처 및 근거

ORD 기록
ord-154a63d17b944e44930c9106bd738256
출처 데이터셋
uspto-grants-2000_03
특허 번호
US06037362

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