Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenazine → 2,3-dimethylbenzo(B)phenazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenazine | HCID 4757 | — |
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 2,3-Diaminonaphthalene | HCID 69872 | — |
| 반응물 | 4,5-Dimethyl-1,2-benzoquinone | HCID 12294704 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2,3-dimethylbenzo(B)phenazine | HCID 19350146 | — |
반응 단계
The 2,3-dimethylbenzo(B)phenazine was prepared by the condensation of 2,3-diaminonapthalene with 4,5-dimethyl-1,2-benzoquinone in 4:1 ethanol to acetic acid at reflux for 2 hours. The phenazine was alkylated by the procedure of Synthesis Example 8, using iodomethane. Electrochemical analysis was consistent with an N,N'-dialkylated phenazine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06037471 |
| 출처 데이터셋 | uspto-grants-2000_03 |
| ORD ID | ord-2a96976d79444bceb26fdc4725a38e3b |
| 출처 메모 | uspto-grants-2000_03 |