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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1637303생성일: 2026년 10월 27일

4-Allyloxybenzoyl chloride → 7-Methacryloyloxy-2-naphthyl 4-allyloxybenzoate

https://huagongshe.com/reaction/1637303

반응식

참여 물질

역할이름HCID투입량
반응물4-Allyloxybenzoyl chlorideHCID 11790137—
반응물2,7-Naphthalenediol monomethacrylateHCID 54509337—
반응물Hydroquinone monomethacrylateHCID 69210285—
용매TriethylamineHCID 8471—
생성물7-Methacryloyloxy-2-naphthyl 4-allyloxybenzoateHCID 1934897295%

반응 단계

In the same way as described in Example 2, 29.5 g (0.15 mol) of 4-allyloxybenzoyl chloride and 34.5 g (0.15 mol) of 2,7-naphthalenediol monomethacrylate (obtainable in a manner similar to that of the hydroquinone monomethacrylate referred to in Example 2 of U.S. Pat. No. 4,604,342) were reacted with triethylamine as acid scavenger. 7-Methacryloyloxy-2-naphthyl 4-allyloxybenzoate, C22H20O5, with an m.p. of 85° C. was obtained in 95% yield. The 1,4-, 1,5- and 2,6-disubstituted naphthalene derivatives can be prepared in the same way.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06040411
출처 데이터셋uspto-grants-2000_03
ORD IDord-ddcdfa0a1195484184ec68d87137acf7
출처 메모uspto-grants-2000_03