Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → 1-(4-Methoxyphenyl)-1,3-dihydro-2H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 1-(4-methoxyphenyl)-1H-indole | HCID 775715 | — |
| 생성물 | 1-(4-Methoxyphenyl)-1,3-dihydro-2H-indol-2-one | HCID 13339544 | — |
반응 단계
Omitting the final chromatography, but triturating the crude product three times with ether, 1-(4-methoxyphenyl)indole (18.1 g, 81 mmoles) was converted to title product, 12.0 g, m.p. 115°-117° C., pnmr/CDCl3 /TMS/delta: 3.65 (s, 2H), 3.8 (s, 3H), 6.6-7.4 (m, 8H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04879391 |
| 출처 데이터셋 | uspto-grants-1989_11 |
| ORD ID | ord-ff26d6f618304204b719f9a9f4303261 |
| 출처 메모 | uspto-grants-1989_11 |