1-Octanol → HCID 15696565, 화합물

반응식

[OH:1][CH:2]1[NH:6][C:5](=[O:7])[CH2:4][CH2:3]1.[CH2:8](O)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[CH2:8]([O:1][CH:2]1[NH:6][C:5](=[O:7])[CH2:4][CH2:3]1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

참가 물질

반응물 2

HCID 9571-Octanol

HCID 1941485-Hydroxy-2-pyrrolidone

생성물 1

HCID 15696565HCID 15696565, 화합물

실험 절차

7.5 g of 5-hydroxy-pyrrolidin-2-one, 10 cm3 of n-octanol and 4 g of Amberlite IR 120H are heated to 60° C. for 4 hours. After filtering, the n-octanol is eliminated by distilling under reduced pressure. 5.5 g of the expected product is obtained, m.p. 36°-38° C., crystallized from hexane.

후처리

filtrationAfter filtering
distillationby distilling under reduced pressure

출처 및 근거

ORD 기록: ord-1f5cd7c854d64e72960378e2514498cf
출처 데이터셋: uspto-grants-1989_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04882350

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