HCID 3760131, 화합물 → HCID 1787923, 화합물
반응식
[C:1]1([CH:7]=[CH:8][C:9]([NH:11][NH:12][C:13]([O:15][CH3:16])=[O:14])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>[Pd].CO>[C:1]1([CH2:7][CH2:8][C:9]([NH:11][NH:12][C:13]([O:15][CH3:16])=[O:14])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
4
실험 절차
22.0 g (0.1 mole) of methyl 3-(β-phenylacryloyl)-carbazate are dissolved in 300 ml. of methanol and the solution is hydrogenated in the presence of 0.2 g. of a palladium-charcoal catalyst. The solution is evaporated. Thus 21.8 g of the white crystalline desired compound are obtained. Yield: 98.2%. M.p.: 118° C.
후처리
- customThe solution is evaporated
출처 및 근거
- ORD 기록
- ord-6988742cf2144b8e85ad210f21489b97
- 출처 데이터셋
- uspto-grants-1989_11
- 특허 번호
- US04883907
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