Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → Phenyl 6-methoxypyridin-3-ylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Phenyl chloroformate | HCID 15891 | — |
| 반응물 | 6-Methoxy-3-pyridinylamine | HCID 81121 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | Phenyl 6-methoxypyridin-3-ylcarbamate | HCID 20185962 | — |
반응 단계
5-amino-2-methoxy-pyridine (30 mg, 0.24 mmol) and potassium carbonate (167 mg, 1.20 mmol) are dissolved in N-methyl 2-pyrrolidone (1 ml). Phenyl chloroformate (36 μl, 0.29 mmol) is added and the reaction mixture is stirred at room temperature for 2 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08114877B2 |
| 출처 데이터셋 | uspto-grants-2012_02 |
| ORD ID | ord-42d223cffd164cefbcf61fcc22d3a9e6 |
| 출처 메모 | uspto-grants-2012_02 |