Thionyl Chloride → HCID 59540922, 화합물

HRID 1642084노트

반응식

[CH2:1]([O:8][CH:9]1[CH2:14][CH2:13][C:12]([CH3:18])([C:15](O)=[O:16])[CH2:11][CH2:10]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.S(Cl)([Cl:21])=O>>[CH2:1]([O:8][CH:9]1[CH2:14][CH2:13][C:12]([CH3:18])([C:15]([Cl:21])=[O:16])[CH2:11][CH2:10]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 59540962HCID 59540962, 화합물

생성물 1

HCID 59540922HCID 59540922, 화합물수율 99%

실험 절차

A solution of 4-benzyloxy-1-methyl-cyclohexanecarboxylic acid (1.71 g, 6.89 mmol) in thionyl chloride (10 ml) was refluxed for 2 hours. The reaction mixture was concentrated on high vacuum giving 1.84 g (99%) of 4-benzyloxy-1-methyl-cyclohexanecarbonyl chloride as a yellow oil.

후처리

concentrationThe reaction mixture was concentrated on high vacuum

출처 및 근거

ORD 기록: ord-8b268db02d4149128dddb5fc29c8dfeb
출처 데이터셋: uspto-grants-2012_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08119636B2

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