참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4-Aminobenzonitrile | HCID 13396 | — |
| 반응물 | 2-Amino-4,6-dichloropyrimidine | HCID 65522 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-[(2-Amino-6-chloropyrimidin-4-yl)amino]benzonitrile | HCID 240806 | — |
반응 단계
300 mg (1.83 mmol) of 2-amino-4,6-dichloropyrimidine and 216 mg (1.83 mmol) of 4-aminobenzonitrile are suspended in 6 ml of water. 180 μl of concentrated hydrochloric acid are added, and the mixture is stirred at 100° C. overnight. The precipitate is filtered off with suction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07737153B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-b294971d5690468ca48fed2a90495ae2 |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
