HCID 57583245, 화합물 → HCID 57583271, 화합물
반응식
[CH2:1]([N:8](C)[CH2:9][CH2:10][CH:11]([CH2:24][N:25](CC1C=CC=CC=1)[CH3:26])[CH2:12][CH2:13][CH2:14][N:15](CC1C=CC=CC=1)[CH3:16])C1C=CC=CC=1.[H][H]>[Pd]>[CH3:1][NH:8][CH2:9][CH2:10][CH:11]([CH2:24][NH:25][CH3:26])[CH2:12][CH2:13][CH2:14][NH:15][CH3:16]참가 물질
4
실험 절차
To a methanolic solution of N1,N6-Dibenzyl-3-[(benzyl-methyl-amino)-methyl]-N1,N6-dimethylhexane-1,6-diamine (1 g, 0.002 mol) was added 1 g of Pd/C. The solution was exposed to 2 bar of hydrogen and left to shake for 48 hours at ambient temperature. The reaction mixture was filtered through celite and concentrated at reduced pressure to yield a viscous oil. The structure was confirmed by NMR, yield ˜90%.
후처리
- waitleft
- filtrationThe reaction mixture was filtered through celite
- concentrationconcentrated at reduced pressure
- customto yield a viscous oil
출처 및 근거
- ORD 기록
- ord-bfefebd5575f43ba94aafc55c2774683
- 출처 데이터셋
- uspto-grants-2012_02
- 특허 번호
- US08124806B2
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