Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(1,3-Dioxan-2-yl)methanol → 2-(((4-(1,3-Dioxan-2-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (1,3-Dioxan-2-yl)methanol | HCID 142350 | — |
| 반응물 | 2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776002 | — |
| 생성물 | 2-(((4-(1,3-Dioxan-2-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66775693 | 10% |
반응 단계
The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 1,3-dioxan-2-ylmethanol obtained in the step (32b) to obtain the title compound (148 mg, total yield: 10%) as a light yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08124780B2 |
| 출처 데이터셋 | uspto-grants-2012_02 |
| ORD ID | ord-3b3295f9cbd447d5abec97debf851a36 |
| 출처 메모 | uspto-grants-2012_02 |