Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-oxo-2,3-dihydro-1H-indene-5-carbonitrile → 1-hydroxy-2,3-dihydro-1H-indene-5-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-oxo-2,3-dihydro-1H-indene-5-carbonitrile | HCID 312896 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | 1-hydroxy-2,3-dihydro-1H-indene-5-carbonitrile | HCID 14515323 | — |
반응 단계
The operation is carried out as in preparation 10, starting with 5-cyano-1-indanone (1.93 g), the extracted residue is taken up in 20 ml of hexane, with agitation for one hour. After filtering, the filtrate is dried at 45° C. under reduced pressure and 1.92 g is obtained,
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05180741 |
| 출처 데이터셋 | uspto-grants-1993_01 |
| ORD ID | ord-2eae400e965f4daf84e7cb16d725c5d4 |
| 출처 메모 | uspto-grants-1993_01 |