Ammonia → HCID 67810172, 화합물

HRID 1647166노트

반응식

HRID 1647166 반응식
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[C:12](=[O:13])[CH:11]=[CH:10]O[C:8]=1[CH3:14].[NH3:15]>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][O:6][CH:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:15]=[C:8]1[CH3:14]

참가 물질

3

반응물 2

HCID 222AmmoniaHCID 19926461HCID 19926461, 화합물

생성물 1

HCID 67810172HCID 67810172, 화합물수율 100%

실험 절차

A solution of 3-(3-methoxy-1-propoxy)-2-methyl-4-pyrone (0.31 g, 1.7 mmol) in 50 ml concentrated aqueous NH3 was heated to 120° C. for 2 h in an autoclave. The reaction mixture was transferred to a round bottomed flask and evaporation off the solvent afforded 0.32 g (100%) product as a yellow oil.

후처리

  1. customThe reaction mixture was transferred to a round bottomed flask
  2. customevaporation off the solvent

출처 및 근거

ORD 기록
ord-99355f82762f4f9ab9fdd5ee3cbc5650
출처 데이터셋
uspto-grants-1995_07
특허 번호
US05430042

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