참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 4-[[4-chloro-3-(2,2,3,3,3-pentafluoropropoxymethyl)phenyl]hydrazinylidene]-2-phenyl-1,3-oxazol-5-one | HCID 178519063 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Flupoxam | HCID 86353 | — |
반응 단계
A 29% ammonia aqueous solution (8.82 g, 150 mmol) was added to 100 g of water, and to the solution was added 2-phenyl-4,5-oxazoledione 4-[4-chloro-3-(2,2,3,3,3-pentafluoropropoxy)methylphenyl]hydrazone (39.7 g, purity: 97%, water content: 40%, 50 mmol). The mixture was vigorously stirred to produce a slurry. The slurry was heated to 80° C. in a water bath. In the course of the heating, the slurry abruptly changed its color, exhibiting an increase in the viscosity, at 65°-70° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05434268 |
|---|
| 출처 데이터셋 | uspto-grants-1995_07 |
|---|
| ORD ID | ord-b2a9fd777acf499687b4271b2c5eaa04 |
|---|
| 출처 메모 | uspto-grants-1995_07 |
|---|
