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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Potassium Carbonate → [(2,3-Dihydro-3-oxo-1H-naphtho[2,1-b]pyran-8-yl)oxy]acetic Acid 1,1-Dimethylethyl Ester

HRID 1648104
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인쇄 미리보기

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HRID 1648104 반응식
[OH:1][C:2]1[CH:3]=[C:4]2[C:13](=[CH:14][CH:15]=1)[C:12]1[CH2:11][CH2:10][C:9](=[O:16])[O:8][C:7]=1[CH:6]=[CH:5]2.Br[CH2:18][C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[CH3:23][C:22]([O:21][C:19](=[O:20])[CH2:18][O:1][C:2]1[CH:3]=[C:4]2[C:13](=[CH:14][CH:15]=1)[C:12]1[CH2:11][CH2:10][C:9](=[O:16])[O:8][C:7]=1[CH:6]=[CH:5]2)([CH3:25])[CH3:24]
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참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 79177tert-Butyl bromoacetate2회HCID 199219571,2-Dihydro-8-hydroxy-3H-naphtho[2,1-b]pyran-3-one

생성물 1

HCID 54520651[(2,3-Dihydro-3-oxo-1H-naphtho[2,1-b]pyran-8-yl)oxy]acetic Acid 1,1-Dimethylethyl Ester수율 91%

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

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온도
60 °C

실험 절차

A mixture of 2.18 g (10.2 mmol) of 1,2-dihydro-8-hydroxy-3H-naphtho[2,1-b]pyran-3-one from the preceding example, 4.84 g (24.8 mmol) of t-butyl bromoacetate, 5.63 g (40.7 mmol) of anhydrous granular potassium carbonate and 55.5 mL of 2-butanone was heated at 60° C. for 24 hr. A second portion of t-butyl bromoacetate (0.5 mL, 3.1 mmol) was added and the reaction was allowed to proceed for another 17 hr. After being cooled to room temperature, the mixture was filtered and the solids were washed with ethyl acetate and ether. The filtrate and washes were combined and concentrated in vacuo, and the crude product was flash chromatographed on 360 g of silica gel, eluting with hexane-ethyl acetate (7:1 then 6:1) affording 3.04 g (91.0%) of the title compound as a white solid, mp 95°-96° C.

후처리

  1. temperatureAfter being cooled to room temperature
  2. filtrationthe mixture was filtered
  3. washthe solids were washed with ethyl acetate and ether
  4. concentrationconcentrated in vacuo
  5. customchromatographed on 360 g of silica gel
  6. washeluting with hexane-ethyl acetate (7:1

출처 및 근거

ORD 기록
ord-d966d50141bb4db688e42da38fa61368
출처 데이터셋
uspto-grants-1995_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05434186

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