O-Xylene → HCID 15376513, 화합물
반응식
[C:1]1([C:7]2[C:8](=O)[O:9][C:10](C)(C)[O:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C=[N:17][C:18]([CH3:26])([C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH3:19].[C:27]1(C)C(C)=CC=CC=1>>[CH3:27][C:8]1[O:9][CH2:10][N:17]([C:18]([CH3:26])([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH3:19])[C:12](=[O:11])[C:7]=1[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1참가 물질
4
실험 절차
Xylene (2 ml) was added to a mixture of 5-phenyl-2,2-dimethyl-2H,4H-1,3-dioxin-4-one (0.82 g) and N-methylene-1-methyl-1-phenylethylamine (0.59 g), and the resulting mixture was heated at reflux for 20 minutes for reaction. The reaction mixture was purified by silica gel chromatography to obtain the captioned compound (0.9 g).
후처리
- temperaturethe resulting mixture was heated
- temperatureat reflux for 20 minutes for reaction
- customThe reaction mixture was purified by silica gel chromatography