Butyric Acid → Methylthiomethyl butyrate

HRID 1648896노트

반응식

[C:1]([OH:6])(=[O:5])[CH2:2][CH2:3][CH3:4].[CH3:7][S:8][CH2:9]Cl.C(N(CC)CC)C>>[C:1]([O:6][CH2:7][S:8][CH3:9])(=[O:5])[CH2:2][CH2:3][CH3:4]

참가 물질

반응물 3

HCID 264Butyric Acid

HCID 8471Triethylamine

HCID 16916Chloromethyl methyl sulfide

생성물 1

HCID 3018539Methylthiomethyl butyrate

실험 절차

This product was prepared according to the procedure described in Example 1, by reacting butyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 71°-73° C./12 mm Hg, n20 1.4521.

후처리

customThis product was prepared

출처 및 근거

ORD 기록: ord-46621d5a4dad4506858a28fffd41f5bf
출처 데이터셋: uspto-grants-1983_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04414233

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