Triethylamine → Methylthiomethyl Geranate

HRID 1648907노트

반응식

HRID 1648907 반응식
[C:1]([OH:12])(=[O:11])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4].[CH3:13][S:14][CH2:15]Cl.C(N(CC)CC)C>>[C:1]([O:12][CH2:13][S:14][CH3:15])(=[O:11])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:9])[CH3:10])\[CH3:4]

참가 물질

4

반응물 3

HCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfideHCID 5275520Geranic acid

생성물 1

HCID 86738396Methylthiomethyl Geranate

실험 절차

This product was prepared according to the procedure described in Example 1, by reacting geranic acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 111°-112° C./2 mm Hg, n20 1.4912.

후처리

  1. customThis product was prepared

출처 및 근거

ORD 기록
ord-71fbd4cf77f74978b6eb177cb7227d38
출처 데이터셋
uspto-grants-1983_11
특허 번호
US04414233

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