Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dinitrotoluene → beta-Dipropylamino-2,3-dinitrostyrene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dinitrotoluene | HCID 11761 | — |
| 반응물 | 1-tert-Butoxy-N,N,N',N'-tetrapropylmethanediamine | HCID 13771313 | — |
| 생성물 | beta-Dipropylamino-2,3-dinitrostyrene | HCID 54130656 | 85.8% |
반응 단계
For two hours, 5.5 g of 2,3-dinitrotoluene is heated with 13.0 g of bisdipropylamino-tert-butoxymethane to 60° C. After cooling, the reaction mixture is freed of volatile components under a high vacuum, thus obtaining 7.6 g of β-dipropylamino-2,3-dinitrostyrene as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04925854 |
| 출처 데이터셋 | uspto-grants-1990_05 |
| ORD ID | ord-beb7c777ba3f47c29ea191bf7f02fde5 |
| 출처 메모 | uspto-grants-1990_05 |