3,4-Dihydro-2,2-dimethyl-4-oxo-2H-pyran-6-carboxylic acid → HCID 15009971, 화합물
반응식
[CH3:1][C:2]1([CH3:12])[CH2:7][C:6](=[O:8])[CH:5]=[C:4]([C:9]([OH:11])=[O:10])[O:3]1.[H][H]>O1CCCC1.[C].[Pd]>[CH3:1][C:2]1([CH3:12])[CH2:7][C:6](=[O:8])[CH2:5][CH:4]([C:9]([OH:11])=[O:10])[O:3]1참가 물질
5
실험 절차
In 8 ml of tetrahydrofuran was dissolved 0.5 g of 3,4-dihydro-2,2-dimethyl-4-oxo-2H-pyran-6-carboxylic acid, followed by adding thereto 50 mg of 10% palladium-carbon, and the reaction was carried out with stirring in a hydrogen stream at room temperature for 3 hours.
후처리
- additionby adding
출처 및 근거
- ORD 기록
- ord-3bb3eeeca5364c3a8babb07b9da4c2d1
- 출처 데이터셋
- uspto-grants-1990_05
- 특허 번호
- US04927919
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