HCID 15239992, 화합물 → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
반응식
C([O:8][C:9]1[C:10]([C:18]([O:20][CH3:21])=[O:19])=[N:11][C:12]([N:15]([CH3:17])[CH3:16])=[CH:13][CH:14]=1)C1C=CC=CC=1>[C].[Pd].C(OCC)(=O)C>[CH3:17][N:15]([C:12]1[N:11]=[C:10]([C:18]([O:20][CH3:21])=[O:19])[C:9]([OH:8])=[CH:14][CH:13]=1)[CH3:16]참가 물질
4
실험 절차
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and the mixture was hydrogenated under atmospheric pressure. After completion of the reaction, the product was filtered and concentrated to obtain crystals.
후처리
- customAfter completion of the reaction
- filtrationthe product was filtered
- concentrationconcentrated
- customto obtain crystals
출처 및 근거
- ORD 기록
- ord-119bbbed187147449d212ea1efbaeb9e
- 출처 데이터셋
- uspto-grants-1995_04
- 특허 번호
- US05403816
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