Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Butyl isothiocyanate → 1-(3-Chloro-2-methylphenyl)-4-(1-methylpropyl)thiosemicarbazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Butyl isothiocyanate | HCID 78151 | — |
| 반응물 | (3-Chloro-2-methylphenyl)hydrazine | HCID 702863 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-(3-Chloro-2-methylphenyl)-4-(1-methylpropyl)thiosemicarbazide | HCID 20079515 | — |
반응 단계
1.44 g (10 mmole) of sec-butyl isothiocyanate were added to 1.56 g (10 mmole) of 3-chloro-2-methylphenyl hydrazine dissolved in 120 ml of toluene, and the mixture was refluxed for 2 hours and then evaporated. The remanence was stirred with a small amount of hexane, separated by filtration and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05405857 |
| 출처 데이터셋 | uspto-grants-1995_04 |
| ORD ID | ord-9f0ca789e649440ebae0831a8fd3777f |
| 출처 메모 | uspto-grants-1995_04 |