참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Butanol | HCID 263 | — |
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | 1,2-Dihydroxypropane dodecyl sulfide | HCID 86739775 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1,2-Dihydroxypropane dodecyl sulfide borate | HCID 86748627 | — |
반응 단계
A solution of 1,2-dihydroxypropane dodecyl sulfide (60 g), prepared as described in Example 3, n-butanol (40 g), and toluene (40 g) was heated to 55° C. and 9 g of boric acid were added. The expected amount of water was removed by azeotropic distillation with a maximum reaction temperature of 110° C. The reaction solution was filtered through diatomaceous earth. Solvent was removed by high speed rotary evaporation under reduced pressure yielding a white, waxy solid product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05407451 |
|---|
| 출처 데이터셋 | uspto-grants-1995_04 |
|---|
| ORD ID | ord-165047ad3b1f49ccbd162eb3b62972cc |
|---|
| 출처 메모 | uspto-grants-1995_04 |
|---|
