Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Cyclohexanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Cyclohexene | HCID 8079 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Cyclohexanol | HCID 7966 | — |
| 생성물 | Cyclohexyl acetate | HCID 12146 | — |
반응 단계
Japanese Patent Application Laid-open No. 313447/1989 discloses an addition reaction of acetic acid with cyclohexene in the presence of both ZSM-5, a high silica content-zeolite, as a catalyst and water. According to this method, the reaction temperature is 120° C. and the reaction time is 4 hours resulting in the formation of cyclohexanol in a 12.5% yield and cyclohexyl acetate at most in a 65% yield. The reaction temperature is high and the catalytic activity is low.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05254721 |
| 출처 데이터셋 | uspto-grants-1993_10 |
| ORD ID | ord-96fbb1c681c049e4938f24f20345ff54 |
| 출처 메모 | uspto-grants-1993_10 |