Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Magnesium peroxide (Mg(O2)) → Ethyl 3-ethyl-2-oxo-3-butenoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Magnesium peroxide (Mg(O2)) | HCID 61745 | — |
| 반응물 | Ethyl 3-ethyl-2-hydroxy-3-butenoate | HCID 21529903 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Ethyl 3-ethyl-2-oxo-3-butenoate | HCID 21529899 | — |
반응 단계
16 g of magnesium dioxide were added to a solution of 3.2 g of ethyl 3-ethyl-2-hydroxy-3-butenoate in 65 ml of methylene chloride and the mixture was stirred at room temperature for 11/2 hours. and was filtered. The solvent was distilled from the filtrate under reduced pressure to obtain ethyl 3-ethyl-2-oxo-3-butenoate in the form of a colorless liquid soluble in ether and alcohols and slighly soluble in water.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03962223 |
| 출처 데이터셋 | uspto-grants-1976_06 |
| ORD ID | ord-f6cb125f4bc7477dac862ace69b75d15 |
| 출처 메모 | uspto-grants-1976_06 |