Butylamine → HCID 178514954, 화합물

HRID 1658850노트

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HRID 1658850 반응식
[N+:1]([C:4]1[CH:17]=[CH:16][CH:15]=[C:14]2[C:5]=1[C:6](=[O:19])[CH:7]1[CH:12]([C:13]2=[O:18])[CH2:11][CH:10]=[CH:9][CH2:8]1)([O-])=[O:2].C(N)CCC>C1(C)C=CC=CC=1>[OH:2][NH:1][C:4]1[C:5]2[C:6](=[O:19])[C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[C:13](=[O:18])[C:14]=2[CH:15]=[CH:16][CH:17]=1

참가 물질

4

반응물 2

HCID 8007ButylamineHCID 108689405-Nitro-1,4,4a,9a-tetrahydroanthraquinone

생성물 1

HCID 178514954HCID 178514954, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

반응 조건

온도
70 °C

실험 절차

A mixture of 5.0 parts of 5-nitro-1,4,4a,9a-tetrahydroanthraquinone with 80 parts of toluene and 1.0 part of n-butylamine was stirred at 70°C for 2 hours. The mixture was then distilled under a reduced pressure of 100 mm Hg to remove toluene, washed with 50 parts of methanol and dried under reduced pressure to obtain 4.4 parts of 1-hydroxylaminoanthraquinone.

후처리

  1. distillationThe mixture was then distilled under a reduced pressure of 100 mm Hg
  2. customto remove toluene
  3. washwashed with 50 parts of methanol
  4. customdried under reduced pressure

출처 및 근거

ORD 기록
ord-b3584de3cd3b4e89ac040e3cef6b4bc3
출처 데이터셋
uspto-grants-1976_06
특허 번호
US03966775

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