참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | beta-(2'-Chloro-4-biphenylyl)propionic acid | HCID 1394276 | — |
| 생성물 | beta-(2'-Chloro-4-biphenylyl)propionyl chloride | HCID 21526230 | — |
반응 단계
β-(2'-chloro-4-biphenylyl)propionic acid (26 g.) is treated with thionyl chloride (18 g.) at 0°-5°C. After 10 mins the temperature is raised to 60°C for 30 mins, then the residue is distilled at 0.05 mm to give β-(2'-chloro-4-biphenylyl)propionyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03966801 |
|---|
| 출처 데이터셋 | uspto-grants-1976_06 |
|---|
| ORD ID | ord-1cf2ddcaced44d57af0b1b597587984a |
|---|
| 출처 메모 | uspto-grants-1976_06 |
|---|
