참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethanolamine | HCID 700 | — |
| 반응물 | Lauric Acid | HCID 3893 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Lauric acid monoethanolamide | HCID 8899 | — |
반응 단계
To a solution of 24 g (0.4 mole) ethanolamine in 100 ml toluene was added 40 g (0.2) lauric acid at 50° C. The mixture was refluxed for 6 hours. Toluene was gradually removed to increase the final pot temperature to 140° C. The distillate was collected in a Stark & Dean trap. The toluene was removed by vacuum stripping and the residue was crystallized from n-hexane. The title compound (44 g) thus obtained melted at 80°-84° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04305868 |
|---|
| 출처 데이터셋 | uspto-grants-1981_12 |
|---|
| ORD ID | ord-891d879642f2463097f63866a9287d86 |
|---|
| 출처 메모 | uspto-grants-1981_12 |
|---|
