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Acrylamide → HCID 86738175, 화합물

HRID 1660300
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인쇄 미리보기

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HRID 1660300 반응식
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH2:18][CH:19]=[CH2:20])[CH:10]=[CH:11][CH:12]=[C:13]([C:16]#[N:17])[C:14]#[N:15])[CH:7]=[CH2:8]>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH:10]=[CH:11][CH:12]=[C:13]([C:14]#[N:15])[C:16]#[N:17])[CH2:18][CH:19]=[CH2:20])[CH:7]=[CH2:8]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 6579AcrylamideHCID 53724731{3-[Di(prop-2-en-1-yl)amino]prop-2-en-1-ylidene}propanedinitrile

생성물 1

HCID 86738175HCID 86738175, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A solution of 40 g. of acrylamide, 52 g. of 3-diallylaminoallylidenemalononitrile (A) in 900 cc. of ethanol was refluxed. 1.3 g. of AZBN was added and the solution refluxed for two hours. At two hour time intervals, the following solutions were added in this order by refluxing:

후처리

  1. additionof AZBN was added
  2. temperaturethe solution refluxed for two hours
  3. additionthe following solutions were added in this order
  4. temperatureby refluxing

출처 및 근거

ORD 기록
ord-a20e085380b54c7fbce2344106db85a8
출처 데이터셋
uspto-grants-1981_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04307184

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