Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfur trioxide → 2-(4-Methylphenyl)-2-sulphoacetyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfur trioxide | HCID 24682 | — |
| 반응물 | 2-(4-Methylphenyl)acetyl chloride | HCID 2760634 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2-(4-Methylphenyl)-2-sulphoacetyl chloride | HCID 20556805 | — |
반응 단계
A solution of 4-methylphenylacetyl chloride (1.69 g, 10 mmole) in dichloromethane (20 ml) was treated with a suspension of sulphur trioxide--dioxane complex (15 mmole) in dichloromethane. The mixture was stirred at room temperature for eighteen hours and evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04308259 |
| 출처 데이터셋 | uspto-grants-1981_12 |
| ORD ID | ord-35d560aac5b84defb7eaee8375b6e182 |
| 출처 메모 | uspto-grants-1981_12 |