Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178418437, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | HCID 178418347 | HCID 178418347 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | HCID 178418437 | HCID 178418437 | — |
반응 단계
A solution of 0.39 g (0.001 mol) of trans-O-(4-chlorophenylacetyl)-4-(4-dimethylaminomethylphenyl)-cyclohexanol in 10 ml of diethyl ether is combined at ambient temperature, with stirring, with a 1.5 times equimolar amount of hydrogen chloride in isopropanol added dropwise. The precipitate formed is left for 1 hour at ambient temperature, suction filtered, washed repeatedly with diethyl ether and dried. White crystals are obtained, melting point 231°-233° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05726205 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-cf6dff211f2249548afbc224153b66a4 |
| 출처 메모 | uspto-grants-1998_03 |