Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → 2-[4-(1-Naphthyl)-1-piperazinyl]ethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 2-{2-[4-(1-Naphthyl)-1-piperazinyl]ethyl}-1H-isoindole-1,3(2H)-dione | HCID 21096932 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-[4-(1-Naphthyl)-1-piperazinyl]ethanamine | HCID 4742497 | — |
반응 단계
0.17 ml (3.55 mmol) of hydrazine monohydrate is added slowly at room temperature to a solution of 1.14 g (2.96 mmol) of 2-{2-[4-(1-naphthyl)-1-piperazinyl]ethyl}-1H-isoindole-1,3(2H)-dione, prepared in step 1.1, in 15 ml of ethanol. The reaction mixture is then refluxed for 1 hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08034818B2 |
| 출처 데이터셋 | uspto-grants-2011_10 |
| ORD ID | ord-208174d1adcc4ea1a55049b72803ef09 |
| 출처 메모 | uspto-grants-2011_10 |