Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 3-Bromo-4-hydroxy-5-nitrobenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 3-Bromo-4-hydroxybenzaldehyde | HCID 76308 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 3-Bromo-4-hydroxy-5-nitrobenzaldehyde | HCID 1494378 | — |
반응 단계
3-Bromo-4-hydroxybenzaldehyde (250 mg) was dissolved in 5 ml of acetic acid. Nitric acid (52 μl) was added and the mixture was stirred for 3 h during which a solid formed. The solid was filtered off, washed with water and dried in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08034945B2 |
| 출처 데이터셋 | uspto-grants-2011_10 |
| ORD ID | ord-1f5b60dd7fee4c75b87a95ec00faca54 |
| 출처 메모 | uspto-grants-2011_10 |