Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Mupirocin Calcium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Bactroban | HCID 6435927 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Mupirocin Calcium | HCID 5282317 | — |
반응 단계
Amorphous mupirocin calcium (5.00 g, 4.80 mmole) was dissolved in methanol (15 ml) and stirred to give a clear solution. Water (10 ml) was added to the solution. Methanol from the solution was evaporated at reduced pressure to give a final volume of 7 ml. The mupirocin calcium solution was allowed to crystallize for 60 h at 5° C. The crystalline product was filtered and washed with water (5 ml). The product was dried at 30° C. for 12 h.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737177B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-ec4f4bb3bf064bed92ba29c1ae4fe37f |
| 출처 메모 | uspto-grants-2010_06 |