Dibenzofuran → 3-Nitrodibenzofuran
반응식
[CH:1]1[C:9]2[C:8]3[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=3[O:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[N+:14]([O-])([OH:16])=[O:15]>C(O)(=O)C>[N+:14]([C:3]1[CH:2]=[CH:1][C:9]2[C:8]3[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=3[O:6][C:5]=2[CH:4]=1)([O-:16])=[O:15]참가 물질
4
반응 조건
- 온도
- 65 °C
실험 절차
Combine dibenzofurane (20.0 g, 0.11 mol) and acetic acid (80 ml). Heat to 65° C. Add 98% nitric acid (20.0 g, 11.8 mol). After 3 hours, cool to room temperature to give a solid. Collect the solid by filtration, rinse with water, and dry to give the title compound.
후처리
- temperaturecool to room temperature
- customto give a solid
- customCollect the solid
- filtrationby filtration
- washrinse with water
- customdry
출처 및 근거
- ORD 기록
- ord-65c9d18dcd1e4b979d097492ee7e69f4
- 출처 데이터셋
- uspto-grants-2011_10
- 특허 번호
- US08044090B2
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