Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → Sulfo-n-hydroxysulfosuccinimide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | N-Hydroxysulfosuccinimide | HCID 133909 | — |
| 반응물 | 11-Pyrrol-1-yl-undecanoic acid | HCID 67349574 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Sulfo-n-hydroxysulfosuccinimide | HCID 11254355 | — |
반응 단계
The following are introduced into a 25 ml round-bottomed flask, in order: 11-(1-pyrrolyl)undecan-1-oic acid (2 mmol; 503 mg), of N-hydroxysulphosuccinimide (2 mmol; 434 mg) and dicyclohexylcarbodiimide (DCC) (2.4 mmol; 495 mg). 10 ml of dimethylformamide (DMF) are subsequently added. A cloudy mixture is obtained, which is subjected to magnetic stirring overnight.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07998726B2 |
| 출처 데이터셋 | uspto-grants-2011_08 |
| ORD ID | ord-a380c7e186dc4840827cf64bcae7c453 |
| 출처 메모 | uspto-grants-2011_08 |