Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoate → 4-(Benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoate | HCID 67342913 | — |
| 용매 | Trifluoroacetic acid | HCID 6422 | — |
| 생성물 | 4-(Benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acid | HCID 57879410 | — |
반응 단계
10 mL of trifluoroacetic acid was added to the obtained tert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and methanol was added to the obtained residue and a solid substance was separated by filtration to obtain 31 mg of 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acid as white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07999132B2 |
| 출처 데이터셋 | uspto-grants-2011_08 |
| ORD ID | ord-9aa7eda3a966471e8efde12db1382b51 |
| 출처 메모 | uspto-grants-2011_08 |