Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Vinyl Acetate → HCID 178525781, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Vinyl Acetate | HCID 7904 | — |
| 반응물 | 4-Hydroxycyclohexyl benzoate | HCID 238109 | — |
| 용매 | Diisopropyl Ether | HCID 7914 | — |
| 생성물 | HCID 178525781 | HCID 178525781 | 46% |
반응 단계
To a solution of 4-hydroxycyclohexyl benzoate (81.5 g) and Lipase QLG (40 g) in diisopropyl ether (800 mL) was added vinyl acetate (120 mL) at room temperature. After being stirred at room temperature for 2 hr, Lipase QLG was filtered off. The filtrate was concentrated under reduced pressure. The residue was purified by silica gel column chromatography to give the title compound as a colorless solid (37.5 g, 46%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07998968B2 |
| 출처 데이터셋 | uspto-grants-2011_08 |
| ORD ID | ord-9452e169fac44bedba91133d72773432 |
| 출처 메모 | uspto-grants-2011_08 |