Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluoroanisole → 5-Fluoro-2-methoxybenzene-1-sulfonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluoroanisole | HCID 9987 | — |
| 반응물 | Chlorosulfonic acid | HCID 24638 | — |
| 생성물 | 5-Fluoro-2-methoxybenzene-1-sulfonyl chloride | HCID 2783409 | — |
반응 단계
4-Fluoroanisole (10.0 g) was carefully added to chlorosulphonic acid (45.81 g) at 0° C. The mixture was stirred at RT for 2 h, then quenched with ice-water (500 ml) and the solid filtered and dried, yield 16.50 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08003703B2 |
| 출처 데이터셋 | uspto-grants-2011_08 |
| ORD ID | ord-f4c08e0fa871485eb64cd4a4f57de450 |
| 출처 메모 | uspto-grants-2011_08 |