Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Ferulate → Methyl 3-(4-hydroxy-3-methoxyphenyl)propanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Ferulate | HCID 5357283 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 3-(4-hydroxy-3-methoxyphenyl)propanoate | HCID 523498 | 101.9% |
반응 단계
To a solution of methyl (E)-3-(4-hydroxy-3-methoxyphenyl)-2-propenoate (3.0 g, 14 mmol) in methanol (30 mL) was added 10% palladium carbon (50% water content, 0.20 g), and the mixture was stirred at room temperature for 4 hours under hydrogen atmosphere. The reaction solution was filtered, and then the filtrate was concentrated under reduced pressure to give the title compound (3.0 g, yield 97%) as an oily matter. The obtained compound was used in the next reaction without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08008525B2 |
| 출처 데이터셋 | uspto-grants-2011_08 |
| ORD ID | ord-1c795cb626f94a5da44697cc230bba21 |
| 출처 메모 | uspto-grants-2011_08 |