(+-)-4-Methylhexanoic acid → HCID 12600624, 화합물

반응식

[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5](O)=[O:6].S(Cl)([Cl:12])=O>>[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5]([Cl:12])=[O:6]

참가 물질

반응물 2

HCID 15271(+-)-4-Methylhexanoic acid

HCID 24386Thionyl Chloride

생성물 1

HCID 12600624HCID 12600624, 화합물

실험 절차

The acid from step A2 is converted into the acid chloride by interaction with thionyl chloride according to a standard method. After removal of the excess of thionyl chloride, the residual acid chloride is used in step C2 without further purification.

후처리

customAfter removal of the excess of thionyl chloride
customthe residual acid chloride is used in step C2 without further purification

출처 및 근거

ORD 기록: ord-677e682bdd7c48c3b1e43681e0ff2d2d
출처 데이터셋: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04077260

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