3-Chlorophenoxazine → 3-Chloro-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

반응식

[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[NH:6][C:7]3[C:12]([O:13][C:14]=2[CH:15]=1)=[CH:11][CH:10]=[CH:9][CH:8]=3.Cl.[NH:17]1[CH2:21][CH2:20][CH:19]=[CH:18]1>>[ClH:1].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:6]([C:18]3[N:17]([C:18]4[CH2:19][CH2:20][CH2:21][N:17]=4)[CH2:21][CH2:20][CH:19]=3)[C:7]3[C:12]([O:13][C:14]=2[CH:15]=1)=[CH:11][CH:10]=[CH:9][CH:8]=3

참가 물질

반응물 2

HCID 189139213-Chlorophenoxazine

HCID 23318315Pyrroline hydrochloride

생성물 1

HCID 203071793-Chloro-10-[1-(1-pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

실험 절차

Reaction of 3-chlorophenoxazine with 2-chloro-(1-pyrrolin-;b 2-yl)pyrroline hydrochloride according to the procedure of Example 7 affords 3-CHLORO-10-[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]PHENOXAZINE HYDROCHLORIDE, m.p. 262.5°-270° C. (dec.) (corr.), from ethanol-ether.

출처 및 근거

ORD 기록: ord-debeab51bb1443bcb6ef08e2ccfe7ab3
출처 데이터셋: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04077959

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