Ethanolamine → HCID 2727773, 화합물

HRID 1678879노트

반응식

[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][OH:6].C(CN)O.OCCN1[C:23](=[O:24])[C:22]2[CH:25]=[CH:26][CH:27]=[C:20]3[C:21]=2[C:16](=[CH:17][CH:18]=[CH:19]3)[C:15]1=[O:28]>>[OH:6][CH2:5][CH2:4][CH2:3][CH2:2][N:1]1[C:15](=[O:28])[C:16]2[CH:17]=[CH:18][CH:19]=[C:20]3[C:21]=2[C:22](=[CH:25][CH:26]=[CH:27]3)[C:23]1=[O:24]

참가 물질

반응물 3

HCID 700Ethanolamine

HCID 258684-Amino-1-butanol

HCID 223681NSC 11547

생성물 1

HCID 2727773HCID 2727773, 화합물

실험 절차

Following the procedure of example 1(a) and (b) but substituting 4-aminobutanol for the ethanolamine in part (a) one obtains 2-(4-hydroxybutyl)-1H-benz[de]isoquinoline-1,3(2H)-dione, 4-methylbenzenesulfonate ester.

출처 및 근거

ORD 기록: ord-affc93f20e494d32baad64d5f3d14440
출처 데이터셋: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04077958

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