Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → 5-Benzyloxy-2,2-dimethyl-1,3-dioxane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5-Benzyloxy-2,2-dimethyl-1,3-dioxane | HCID 20364889 | — |
반응 단계
Using the procedure of Example 51, 2-benzyloxy-1,3-propanediol and acetone were reacted, using benzene as solvent, to give, after distillation using a short path column, 5-benzyloxy-2,2-dimethyl-1,3-dioxane. The nmr spectrum was consistent with the assigned structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04077982 |
| 출처 데이터셋 | uspto-grants-1978_03 |
| ORD ID | ord-80f56de90df74adaade2cd08e85c9ee3 |
| 출처 메모 | uspto-grants-1978_03 |