Diglyme → HCID 178420510, 화합물

HRID 1679040

반응식

HRID 1679040 반응식
C([N:7]1[C:11]2[N:12]=[CH:13][C:14]3[C:15]([O:23][C:24]4[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=4)=[N:16][C:17]4[N:18]([N:20]=[CH:21][N:22]=4)[C:19]=3[C:10]=2[CH:9]=[N:8]1)C1OC=CC=1.COCCOCCOC.[Se](=O)=O>>[C:24]1([O:23][C:15]2[C:14]3[CH:13]=[N:12][C:11]4[NH:7][N:8]=[CH:9][C:10]=4[C:19]=3[N:18]3[N:20]=[CH:21][N:22]=[C:17]3[N:16]=2)[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=1

참가 물질

4

반응물 3

HCID 8150DiglymeHCID 24007Selenium DioxideHCID 227585308-furfuryl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine

생성물 1

HCID 178420510HCID 178420510, 화합물

실험 절차

0.01 mol. of 8-furfuryl-5-phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine is heated in 50 ml. of diethyleneglycol dimethyl ether containing 0.01 mol. of selenium dioxide at reflux temperature with stirring for two hours. The mixture is filtered hot and evaporated to dryness. 5-Phenyloxy-8H-pyrazolo[4',3':5,6]pyrido[3,4-e][1,2,4]triazolo[1,5-a]pyrimidine remains.

후처리

  1. filtrationThe mixture is filtered hot
  2. customevaporated to dryness

출처 및 근거

ORD 기록
ord-5bacc5ef9b764caaa57482a79a0efa92
출처 데이터셋
uspto-grants-1978_03
특허 번호
US04078064

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