HCID 178463890, 화합물 → HCID 178463877, 화합물

HRID 1679267노트

반응식

HRID 1679267 반응식
[OH:1][C:2]1[CH:7]=[C:6]([CH2:8]C(O)=O)[N:5]=[C:4]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[N:3]=1>C(O)C>[OH:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]=[C:4]([N:12]([CH2:13][CH3:14])[CH2:15][CH3:16])[N:3]=1

참가 물질

3

반응물 1

HCID 178463890HCID 178463890, 화합물

생성물 1

HCID 178463877HCID 178463877, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

4-Hydroxy-2-diethylaminopyrimidin-6-yl acetic acid (4.0 g) was suspended in ethanol (50 ml) and the mixture refluxed for 16 hours. The volatile portion of the mixture was then evaporated under reduced pressure to yield 4-hydroxy-2-diethylamino-6-methyl pyrimidine as a white powder, melting at 135° C.

후처리

  1. temperaturethe mixture refluxed for 16 hours
  2. customThe volatile portion of the mixture was then evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-3f7a19b4e9aa45d08b52f63ed0edecf2
출처 데이터셋
uspto-grants-1978_03
특허 번호
US04080326

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