1,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl- → HCID 70575974, 화합물

HRID 1679495노트

반응식

HRID 1679495 반응식
[Cl:1]N1C(=O)NC(=O)N(Cl)C1=O.[Na].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][N:15]1[CH3:23]>CO>[Cl-:1].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][NH+:15]1[CH3:23]

참가 물질

4

반응물 2

HCID 1816881,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl-HCID 86657659Sodium dichlorocyanuric acid

생성물 1

HCID 70575974HCID 70575974, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

17.8 g (0.1 mol) of sodium dichlorocyanuric acid are added to 15.7 g (0.1 mol) of 2,4-dioxo-hexahydro-1,3,5-trimethyl-s-triazine in 50 ml of methanol and the mixture is stirred. The cyanuric acid which has precipitated is then filtered off and the filtrate is evaporated. The residue which remains on evaporation is digested with water. After renewed filtration to remove residual cyanuric acid, an aqueous solution of the same compound as in Example g is obtained.

후처리

  1. customThe cyanuric acid which has precipitated
  2. filtrationis then filtered off
  3. customthe filtrate is evaporated
  4. customThe residue which remains on evaporation
  5. filtrationfiltration
  6. customto remove residual cyanuric acid
  7. customan aqueous solution of the same compound as in Example g is obtained

출처 및 근거

ORD 기록
ord-3769b7e41fcb49179062e8fdcf5f8766
출처 데이터셋
uspto-grants-1978_03
특허 번호
US04080502

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