Methylamine → HCID 12876310, 화합물
반응식
[CH3:1][C:2]1([C:15]([O:17]C)=O)[C:7]2[NH:8][C:9]3[C:14]([C:6]=2[CH2:5][CH2:4][NH:3]1)=[CH:13][CH:12]=[CH:11][CH:10]=3.[CH3:19][NH2:20]>C(O)C>[CH3:1][C:2]1([C:15]([NH:20][CH3:19])=[O:17])[C:7]2[NH:8][C:9]3[C:14]([C:6]=2[CH2:5][CH2:4][NH:3]1)=[CH:13][CH:12]=[CH:11][CH:10]=3참가 물질
4
실험 절차
4.8 g (0.02 mol) of methyl 1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-1-carboxylate are dissolved in 100 ml of ethanol saturated with methylamine. The solution is left at ambient temperature for 48 hours. The solvent is removed and the residue is then taken up in 20 ml of ethanol. The product is filtered off and washed with ethanol.
후처리
- customThe solvent is removed
- filtrationThe product is filtered off
- washwashed with ethanol
출처 및 근거
- ORD 기록
- ord-06199cb348db45458e575e60b24f2ae9
- 출처 데이터셋
- uspto-grants-1981_06
- 특허 번호
- US04272539
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