Sodium Iodide → 3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl iodide
반응식
[CH3:1][C:2](=[CH:6][CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]2[O:15][CH2:16][O:17][C:11]=2[CH:10]=1)[CH2:3][CH2:4]Br.[I-:18].[Na+]>CC(C)=O>[CH3:1][C:2](=[CH:6][CH2:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]2[O:15][CH2:16][O:17][C:11]=2[CH:10]=1)[CH2:3][CH2:4][I:18]참가 물질
4
실험 절차
3-Methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl iodide [VI; Ar is 3,4-methylenedioxyphenyl, R is CH3 ] was prepared from 19.0 g. of 3-methyl-6-(3,4-methylenedioxyphenyl)-3-hexenyl bromide (Preparation C3) and 10.5 g. of sodium iodide in 125 ml. of acetone, to give 21 g. of product as a yellow oil.
출처 및 근거
- ORD 기록
- ord-73c10c39580e4ca2bbfff1f161b10ae3
- 출처 데이터셋
- uspto-grants-1981_06
- 특허 번호
- US04275201
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